Beamline 7.2W
Macromolecular Crystallography
Support Facilities & Equipment
Helium sample chamber for bulk XRF
Helium gas was purged into the acrylic sample chamber to ensure high efficiency in detecting low-mass elements such as sulfur, chlorine, potassium and calcium in XRF detection system. Magnetic sample holder has a travel range of 10 cm to carry a stack of samples.
Helium sample chamber and its holder for XRF measurement
XRF Standard Reference Materials (SRM)
X-ray Fluorescence (XRF) analysis requires precise calibration to ensure accurate elemental measurements. Our facility provides a comprehensive set of Standard Reference Materials (SRMs) for XRF applications, supporting research and quality assurance across various fields such as environmental science, materials engineering, and food safety.
Available XRF Standards
Plant Material
Biological / Animal Tissue
Airborne Particulate / Urban Pollution
Soil / Sediment
Minerals & Rocks
SRM 99b
Soda Feldspar
SRM 70ิb
Potassium Feldspar
SRM 1648a
Urban Particulate Matter
SRM 2709a
San Joaquin Soil
SRM 2702
Inorganics in Marine Sediment
SRM1566b
Oyster Tissue
SRM CD281
Rye Grass
SRM 1573a
Tomato Leaves
SRM 1568b
Rice Flour
SRM 1515
Apple Leaves
SRM 482
Lichen
SRM Code
Description
SRM 2780a
Hard Rock Mine Waste
SRM 688
Basal Rock
SRM 278
Obsidian Rock
Metal and Alloys
NBS No. 1115
Commercial Bronze Standard
SRM 1107
Naval BUNS 46400
NBS No. 1117
Commercial Bronze Standard
NBS No. 1116
Commercial Bronze Standard
SRM 1157
Tool Steel (AISI M2)
SRM 1134
Low-Alloy High Silicon Steel (disk form)
SRM 1763b
Low Alloy Steel (disk form)
SRM 1264a
High-Carbon Steel (Modified) (disk form)
SRM 1230
High-Temperature Alloy A286 (disk form)
Glass
SRM 93a
Borosilicate Glass (12.5% B₂O₃)
SRM 89
Lead-Bariuam Glass
SRM 80a
Soda-Lime Glass (Beads)
32XLB14H
Leaded bronze
32XLB10G
Leaded bronze
SRM 1764a
Low Alloy Steel
SRM 610
Trace Elements in Glass
SRM 606
Trace Elements in Glass
SRM 614
Trace Elements in Glass
SRM 612
Trace Elements in Glass
SRM 616
Trace Elements in Glass
SRM 1411
Soft BorosiliGlass
Helium sample chamber for micro-XRF
For micro-focused X-ray fluorescence measurement of light elements such as sulfur, chlorine, potassium and calcium, sample chamber is purged with inert helium gas to reduce absorption by air. A sample chamber for helium purge is made from polylactic acid (PLA), plant-based thermoplastic polyester.
Helium sample chamber and its holder for micro-XRF measurement
XAS Standard Reference Materials
Our facility provides a comprehensive range of standard reference materials for X-ray Absorption Spectroscopy (XAS) to ensure accurate and reliable measurements. These materials are essential for calibration, verification, and advanced analysis, and include:
✔ Metal Foils – commonly used for energy calibration and edge
position verification.
✔ Standard Compounds – such as nitrides and oxides, ideal for
chemical state analysis and structural studies.
👉 For the complete list of available XAS Standard Reference Materials and their detailed specifications, please visit the official Beamline 1.1W website.
For in-situ X-ray Experiments
Our facility provides advanced equipment for high-temperature, in-situ X-ray studies, including X-ray Absorption Spectroscopy (XAS) and X-ray Diffraction (XRD). These instruments offer precise temperature control, flexible sample environments, and reliable performance, enabling cutting-edge research in phase transformations, structural analysis, and material characterization.
Equipment Overview
Equipment
Temperature Range
Atmosphere Options
Key Features
Octagon Furnace
(In-house development)
25 °C – 700 °C
Ambient
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Supports transmission & fluorescence modes
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Handles high/low concentration samples
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Octagonal design with multiple apertures enabling flexible beam adjustment
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Compact, easy-to-install design
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Computer-controlled heating
Graphite Dome Hot Stage
(Anton Paar GmbH, Austria)
-
25 °C – 1100 °
(Air, Nitrogen, vacuum)
-
25 °C – 1000 °
(Helium)
Vacuum, Air, Nitrogen, Helium
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Phase transformation & structural studies
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Controlled atmospheres
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Up to 1100 °C
-
Computer-controlled precision
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Flexible sample handling
👉 Contact Information
For access or more information, please contact our facility staff.
Sample holder and heat transfer setup inside the Octagon Furnace, including metal block and temperature sensor for in-situ X-ray absorption experiments.
Graphite dome hot stage with sample holder for in-situ measurements
Automated Protein Crystallization System
For Macromolecular Crystallography Analysis
Our Macromolecular Crystallography Facility is equipped with advanced tools and systems to support high-quality crystallographic research. We provide specialized instruments for crystal handling, inspection, and automated crystallization processes.
Crystal Manipulation Tool
To ensure precise and safe handling of crystals during experiments, our facility offers:
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Precision tweezers for delicate crystal handling
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Cryo-cooling systems to maintain low-temperature conditions during data collection
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Goniometer bases (caps) and pins for secure crystal mounting
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High-resolution stereo microscopes for crystal inspection and alignment
These instruments are maintained to the highest standards and are available to all registered users conducting crystallographic experiments.
Specialized instruments for crystal mounting and inspection
Oxford Cryosystems 700 Series
Low-temperature (100K) data collection
Our automated system streamlines the protein crystallization process, enabling high‑throughput screening and reproducibility. Equipped with the Oryx8 Protein Crystallization Robot (Douglas Instruments Ltd., UK), it supports sitting drop and microbatch screening as well as optimization.
👉 Contact Information
For access inquiries, please contact:
Dr. Ratana Charoenwattanasatien
Email: ratana@slri.or.th
Oryx8 Protein Crystallization Robot
High-efficiency automated setup for protein crystallization
